Heterogeneously catalyzed phosphine-free heck cross-coupling reaction of aryl halides with reusable palladium(II) schiff base complex

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Heterogeneously Catalyzed Phosphine-Free Heck Cross-Coupling Reaction of Aryl Halides with Reusable Palladium(II) Schiff Base Complex

O acoplamento entre haletos de arila e terminais alceno (reação de Heck) foi investigado na presença de catalisadores de paládio (II) suportados em poliestirenos contendo bases de Schiff. O catalisador é estável frente ao ar e umidade, e tem atividade catalítica significativa nas reações de acoplamento cruzado de Heck sob condições normais. Vários haletos de arila e alcenos terminais foram faci...

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Transition-Metal-Free Cross-Coupling of Aryl Halides with Arylstannanes.

Transition-metal-free LiCl-promoted cross-coupling reactions of tetraphenyltin, trichlorophenyl-, dichlorodiphenyl-, and chlorotriphenylstannanes with aryl halides in DMF provided access to biaryls in good to high yields. Up to four phenyl groups were transferred from the organostannanes substrates. The aryls bearing electron-withdrawing groups in either halides or organotin substrates gave cou...

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Cobalt-Catalyzed Cross-Coupling Reactions of Aryl Halides

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Palladium(II)-catalyzed Heck reaction of aryl halides and arylboronic acids with olefins under mild conditions

A series of general and selective Pd(II)-catalyzed Heck reactions were investigated under mild reaction conditions. The first protocol has been developed employing an imidazole-based secondary phosphine oxide (SPO) ligated palladium complex (6) as a precatalyst. The catalytic coupling of aryl halides and olefins led to the formation of the corresponding coupled products in excellent yields. A v...

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* corresponding author, e-mail: [email protected] ; tel : (216) 74276400 ; fax : (216) 74274437 ABSTRACT: In this work, we have studied the effect of the halide nature in the coupling of styrene with halide benzene catalysed by palladium acetate or chloride. The activation by a catalyst of phase-transfer type Aliquat-336 improves the reactivity in N, N-dimethylformamide-water mixture. The...

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ژورنال

عنوان ژورنال: Journal of the Brazilian Chemical Society

سال: 2011

ISSN: 0103-5053

DOI: 10.1590/s0103-50532011000200018